1 Reliability and Reproducibility of the Cryogenic Sapphire Oscillator Technology.

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Reliability and Reproducibility of the Cryogenic
Sapphire Oscillator Technology.
Christophe Fluhr, Benoˆ
ıt Dubois, Guillaume Le Tetu], Valerie Soumann],
Julien Paris[, Enrico Rubiola]and Vincent Giordano]
Abstract—The cryogenic sapphire oscillator (CSO) is a highly
specialized machine, which delivers a reference signal exhibiting
the lowest frequency fluctuations. For the best units, the Allan
deviation (ADEV) is σy(τ)<1015 for integration time
between 1and 104s, with a drift <1014 in one day. The
oscillator is based on a sapphire monocrystal resonating at 10
GHz in a whispering-gallery mode, cooled at 6K for highest
Q-factor and zero thermal coefficient. We report on the progress
accomplished implementing eleven CSOs in about 10 years since
the first sample delivered to the ESA station in Argentina. Short-
term stability is improved by a factor of 3-10, depending on
τ, and the refrigerator’s electric power is reduced to 3 kW.
Frequency stability and overall performances are reproducible,
with unattended operation between scheduled maintenance every
two years. The CSO is suitable to scientific applications requiring
extreme frequency stability with reliable long-term operation.
For example, the flywheel for primary frequency standards,
the ground segment of GNSS, astrometry, VLBI, and radio
astronomy stations.
Index Terms—Time and frequency metrology. ultra-stable
oscillators, frequency stability.
I. INTRODUCTION
SHORT term fractional frequency stability in the 1015
range has been demonstrated more than 20 years ago
with the use of high Q-factor microwave dielectric sapphire
resonator cooled near the liquid helium temperature [1], [2].
In the early 2000s, Cryogenic Sapphire Oscillator (CSO)
breakthrough performances and early uses in the field of
Time and Frequency Metrology have been demonstrated with
prototypes still operating within a liquid He bath [3], [4], [5],
[6], [7]. In 2010, at the FEMTO-ST Institute, we demonstrated
for the first time the possibility to use a cryocooler while
maintaining a state-of-the-art frequency stability [8]. Since,
we undertaken large engineering efforts to rationalize the CSO
design and its development, reduce its electrical consumption
and improve its immunity to environmental perturbations [9],
[10], [11], [12].
Currently, there is no competing technology. The closest
are the laser stabilized to a cryogenic Fabry-Perot cavity
Manuscript created October 2022
France Comt´
e Innov, 25000 Besanc¸on, France.
]FEMTO-ST Institute, Dept. of Time and Frequency, Universit´
e de Bour-
gogne and Franche-Compt´
e (UBFC), and Centre National de la Recherche
Scientifique(CNRS), E-mail: giordano@femto-st.fr, Address: ENSMM, 26
Rue de l’Epitaphe, 25000 Besanc¸on, France.
[My Cryo Firm, 94120 Fontenay-sous-Bois, France.
Physics Metrology Division, Istituto Nazionale di Ricerca Metrologica
INRiM, Torino, Italy.
and the Hydrogen maser, but they do not show the best
stability in same region of the σy(τ)plot, and have quite
different “personalities”. The short term frequency stability
achieved by the CSO is today only surpassed by some high-
class laser prototypes stabilized on a cryogenic ultra-stable
Fabry-Perot cavity [13], [14]. Commercial versions based
on a room temperature Ultra-Low Expansion (ULE) optical
cavity approach the short-term CSO frequency stability
but still present a large long term frequency drift, i.e.
1011 1012/day [15], [16]. Moreover, those optical
sources operate generally in the near IR, and then require a
metrological femto-second laser to derive useful signals in
the microwave or the VHF bands.
Our upgraded CSO technology, code named ULISS-2G,
is today sufficiently mature to be offered as a commercial
product consuming only 3 kW and able to run continuously
for year. A simple maintenance operation, which can be
performed by the user, is only required every two years.
In this paper, we present the performance as well as the
operating history of all the CSOs that we have built and
validated since 2009. The objective here is to demonstrate
the reliability and the reproducibility of our CSO technology.
II. FEMTO-ST CSO DESIGN
A block diagram of the CSO is represented in the figure 1.
Monitoring System
Compressor
He
Temp.
Control PULSE
TUBE
ν
0
10 GHz
100 MHz
10 MHz
Data
100 MHz
cooling water
0
Pound
Control Sustaining stage
ν
Cryostat
Phase comparator
Synthesizer
Power
Control
Resonator
Fig. 1. CSO block diagram: we distinguish 3 mains subsets: the ultra-stable
oscillator itself, the frequency synthesizer and the monitoring system.
arXiv:2210.05545v1 [physics.ins-det] 11 Oct 2022
2
The high Q sapphire resonator is maintained near 6K
in a cryostat cooled with an autonomous Pulse-Tube
(PT) cryocooler. The CSO is a Pound-Galani oscillator:
the resonator is used in transmission mode in a regular
oscillator loop, and in reflection mode as the discriminator
of the classical Pound servo. The sustaining stage and the
control electronics are placed at room temperature. The
CSO output signal at the resonator frequency ν0drives
the frequency synthesizer, which eventually delivers several
output frequencies: 10 GHz, 100 MHz and 10 MHz in the
typical implementation. Eventually the synthesizer outputs
can be disciplined at long term on an external 100 MHz
signal coming from an Hydrogen Maser for example. A
monitoring system scrutinizes all the key parameters to
follow the CSO status. The technological choices relating to
the various subsets have already been described in previous
publications to which we refer the reader [17], [18], [19],
[20]. Here we will simply recall the key features, which make
the originality of our design.
A. Sapphire resonator
Fig. 2. Cryogenic sapphire resonator operating on the WGH15,0,0mode at
9.99 GHz.
The cylindrical resonator 54-mm-diameter and 30-mm-height
is made in a high purity sapphire monocrystal (see Fig. 2). It
operates on the quasi-transverse magnetic whispering-gallery
mode WGH15,0,0at ν0= 9.99 GHz ±5MHz. This choice
greatly simplifies the design of the frequency synthesis
(see below). The sapphire resonator frequency shows near
6 K a turnover temperature T0for which the resonator
sensitivity to temperature variations nulls at first order. The
appearance of this turning point results from the presence in
Al2O3of paramagnetic impurities as Cr3+ or Mo3+, whose
concentration are typically well below 1ppm in weight. The
exacte value of T0is specific to each resonator and for high
quality sapphire crystal is typically found between 5and
9K [21]. At T0, the unloaded Q factor can achieve two
billion depending on the sapphire crystal quality and on the
resonator adjustment and cleaning.
The sapphire resonator includes an integral spindle (see
Fig. 2), such that the sapphire piece can be mounted with no
significant fixing stress in the cylinder’s critical circumferential
region, where the WG mode’s field is concentrated. Since
2009, we have ordered more than 25 sapphire resonators from
several high-quality crystal manufacturers that we selected
after preliminary tests on samples. Of these resonators, 17
were actually tested at low temperature. The following figures
show the reproducibility of resonator main characteristics.
1) ν0, resonator frequency:
CA B
9.99
9.98
9.985
Manufacturer
9.995
10
WGH15 mode frequency (GHz)
Fig. 3. WGH15,0,0mode frequency of the tested resonators.
We had set the tolerances on resonator dimensions to
achieve a frequency of 9.99 GHz ±5MHz which simplifies
the design of frequency synthesis (see Sect. II-C ). Only
one among the tested resonators presents a frequency
notably shifted from the expected value at about 9.998 GHz.
Nevertheless, it could be integrated into a CSO by making
some minor modifications to the synthesis.
2) T0, resonator turnover temperature:
ABC
7
Manufacturer
WGH15 mode turnover temperature (K)
4
5
6
8
9
Fig. 4. WGH15,0,0mode turnover temperature of the tested resonators. The
grey zone: 4.6KT08K corresponds to our specification.
The lowest value of the acceptable temperature range
is 4.6K, which is the lowest achievable temperature in
ULISS-2G increased by 0.5 K. It represents the lowest
allowable T0for an effective temperature stabilization. On
摘要:

1ReliabilityandReproducibilityoftheCryogenicSapphireOscillatorTechnology.ChristopheFluhrr,BenoˆtDuboisr,GuillaumeLeTetu],ValerieSoumann],JulienParis[,EnricoRubiola]andVincentGiordano]Abstract—Thecryogenicsapphireoscillator(CSO)isahighlyspecializedmachine,whichdeliversareferencesignalexhibitingthelo...

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